4-(Trifluoromethyl)phenylhydrazine → HCID 21220532, compound

HRID 1584728Notes

Reaction equation

HRID 1584728 reaction equation
Br.O=[C:3]1[CH:12]([CH2:13][C:14]([O:16]C)=O)[CH2:11][CH2:10][C:9]2[CH:8]=[N:7][CH:6]=[CH:5][C:4]1=2.[F:18][C:19]([F:29])([F:28])[C:20]1[CH:25]=[CH:24][C:23]([NH:26][NH2:27])=[CH:22][CH:21]=1>>[F:18][C:19]([F:28])([F:29])[C:20]1[CH:21]=[CH:22][C:23]([N:26]2[C:14](=[O:16])[CH2:13][CH:12]3[C:3]([C:4]4[CH:5]=[CH:6][N:7]=[CH:8][C:9]=4[CH2:10][CH2:11]3)=[N:27]2)=[CH:24][CH:25]=1

Participants

3

Reactant 2

HCID 1362004-(Trifluoromethyl)phenylhydrazineHCID 70281472HCID 70281472, compound

Product 1

HCID 21220532HCID 21220532, compound

Procedure

Prepared according to the method described in Example 1 from methyl 5,6,7,8-tetrahydro-5-oxoisoquinoline-6-acetate hydrobromide and 4-trifluoromethylphenylhydrazine.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-f869f88f083d4cbbbdbb5a9bb7724ac9
Source dataset
uspto-grants-1999_08
Patent number
US05935956

Reaction notes

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