HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53648913, compound → HCID 18545098, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53648913 | HCID 53648913 | — |
| Reactant | 1,1-Dimethylethyl 2-(4-(4-fluorophenyl)-1-piperazinyl)-2-oxo-1-(phenylmethyl)ethylcarbamate | HCID 53804735 | — |
| Product | HCID 18545098 | HCID 18545098 | 65.3% |
Reaction Steps
Using 1,1-dimethylethyl 2-(4-(4-chlorophenyl)-1-piperazinyl)-2-oxo-1-(2-methylpropyl)ethylcarbamate in lieu of 1,1-dimethylethyl 2-(4-(4-fluorophenyl)-1-piperazinyl)-2-oxo-1-(phenylmethyl)ethylcarbamate, the procedure of Reference Example 13 was otherwise repeated to provide 1-(2-amino-4-methyl-1-oxopentyl)-4-(4-chlorophenyl)piperazine hydrochloride (1.50 g, 65.3%) as white crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05935959 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-51e1763d67f14555a1dbaeec27256ad9 |
| Source note | uspto-grants-1999_08 |