HRID1584872

反应详情

EQUATION

反应方程式

HRID 1584872 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Trifluoroacetic acid (9 ml) was added to a solution of 2-amino-N-[(1-tert-butoxycarbonyl-4-piperidyl)methyl]pyridine-3-carboxamide (2.2 g; prepared in a similar manner to that described above) in dichloromethane (50 ml) and the mixture stirred at ambient temperature for 1 hour. The solvent was removed in vacuo to give crude 2-amino-N-(4-piperidylmethyl)pyridine-3-carboxamide trifluoroacetate.

WORKUP

后处理

  1. customprepared in a similar manner to that
  2. customThe solvent was removed in vacuo