HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 21217668, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 3,6-Dichloro-4,5-dimethylpyridazine | HCID 21187505 | — |
| Product | HCID 21217668 | HCID 21217668 | — |
Reaction Steps
0.69 g(0.03 mol) of metallic sodium was dissolved in 100 ml of absolute ethanol and then 5.31 g(0.03 mol) of 3,6-dichloro-4,5-dimethylpyridazine was added thereto and completely dissolved. The reaction solution was stirred for 4 hours at room temperature and then treated according to the same manner as Preparation 5 to obtain the title compound as a pale white crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05942511 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-4ad9ab41fec442f4975e353d7fcb71ab |
| Source note | uspto-grants-1999_08 |