Ethanol → HCID 21217668, compound

HRID 1585984Notes

Reaction equation

HRID 1585984 reaction equation
[Na].[Cl:2][C:3]1[N:4]=[N:5][C:6](Cl)=[C:7]([CH3:10])[C:8]=1[CH3:9].[CH2:12]([OH:14])[CH3:13]>>[CH2:12]([O:14][C:6]1[N:5]=[N:4][C:3]([Cl:2])=[C:8]([CH3:9])[C:7]=1[CH3:10])[CH3:13]

Participants

4

Reactant 3

HCID 702EthanolHCID 5360545SodiumHCID 211875053,6-Dichloro-4,5-dimethylpyridazine

Product 1

HCID 21217668HCID 21217668, compound

Procedure

0.69 g(0.03 mol) of metallic sodium was dissolved in 100 ml of absolute ethanol and then 5.31 g(0.03 mol) of 3,6-dichloro-4,5-dimethylpyridazine was added thereto and completely dissolved. The reaction solution was stirred for 4 hours at room temperature and then treated according to the same manner as Preparation 5 to obtain the title compound as a pale white crystal.

Workup

  1. dissolutioncompletely dissolved
  2. additiontreated
  3. customaccording to the same manner as Preparation 5

Sources & evidence

ORD record
ord-4ad9ab41fec442f4975e353d7fcb71ab
Source dataset
uspto-grants-1999_08
Patent number
US05942511

Reaction notes

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