Allyl Mercaptan → HCID 9881434, compound

Participants

Reaction Steps

0.23 g(0.01 mol) of metallic sodium was dissolved in 100 ml of absolute methanol and then mixed with 0.93 ml (0.01 mol) of allylmercaptan. To this mixture was added 2.13 g(0.01 mol) of 1-ethoxy-4-chloro-5,6,7,8-tetrahydro-phthalazine obtained from Preparation 9. The reaction solution was refluxed for 3 hours and then treated according to the same manner as Example 1 to obtain the title compound as a freezing white crystal.

Provenance & Evidence