Allyl Mercaptan → HCID 10130734, compound

HRID 1585997Notes

Reaction equation

HRID 1585997 reaction equation
[Na].[CH2:2]([SH:5])[CH:3]=[CH2:4].[CH2:6]([O:10][C:11]1[N:12]=[N:13][C:14](Cl)=[CH:15][CH:16]=1)[CH2:7][CH2:8][CH3:9]>CO>[CH2:6]([O:10][C:11]1[N:12]=[N:13][C:14]([S:5][CH2:2][CH:3]=[CH2:4])=[CH:15][CH:16]=1)[CH2:7][CH2:8][CH3:9]

Participants

5

Reactant 3

HCID 13367Allyl MercaptanHCID 2528253-butoxy-6-chloropyridazineHCID 5360545Sodium

Product 1

HCID 10130734HCID 10130734, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

1.15 g(0.05 mol) of metallic sodium was dissolved in 75 ml of absolute methanol and then mixed with 4.98 ml(0.05 mol) of allylmercaptan. To this mixture was added 9.33 g(0.05 mol) of 3-(n-butoxy)-6-chloropyridazine. The reaction solution was refluxed for 24 hours and then treated according to the same manner as Example 1 to obtain the title compound as a pale yellow oil.

Workup

  1. temperatureThe reaction solution was refluxed for 24 hours
  2. additiontreated

Sources & evidence

ORD record
ord-c653d76dda1245b391a28e607699980c
Source dataset
uspto-grants-1999_08
Patent number
US05942511

Reaction notes

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