Allyl Mercaptan → HCID 54556255, compound

HRID 1585998Notes

Reaction equation

HRID 1585998 reaction equation
[Na].[CH2:2]([SH:5])[CH:3]=[CH2:4].[CH3:6][CH:7]([O:10][C:11]1[N:12]=[N:13][C:14](Cl)=[CH:15][CH:16]=1)[CH2:8][CH3:9]>CO>[CH3:6][CH:7]([O:10][C:11]1[N:12]=[N:13][C:14]([S:5][CH2:2][CH:3]=[CH2:4])=[CH:15][CH:16]=1)[CH2:8][CH3:9]

Participants

5

Reactant 3

HCID 13367Allyl MercaptanHCID 5360545SodiumHCID 12285835HCID 12285835, compound

Product 1

HCID 54556255HCID 54556255, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

0.92 g(0.04 mol) of metallic sodium was dissolved in 120 ml of absolute methanol and then mixed with 3.98 ml(0.04 mol) of allylmercaptan. To this mixture was added 7.47 g(0.04 mol) of 3-(2-butoxy)-6-chloropyridazine. The reaction solution was refluxed for 24 hours and then treated according to the same manner as Example 1 to obtain the title compound as a pale yellow oil.

Workup

  1. temperatureThe reaction solution was refluxed for 24 hours
  2. additiontreated

Sources & evidence

ORD record
ord-831ed901d45243d69715083dfb16af79
Source dataset
uspto-grants-1999_08
Patent number
US05942511

Reaction notes

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