Allyl Mercaptan → HCID 21217662, compound

HRID 1585999Notes

Reaction equation

HRID 1585999 reaction equation
[Na].[CH2:2]([SH:5])[CH:3]=[CH2:4].[C:6]([O:10][C:11]1[N:12]=[N:13][C:14](Cl)=[CH:15][CH:16]=1)([CH3:9])([CH3:8])[CH3:7]>CO>[C:6]([O:10][C:11]1[N:12]=[N:13][C:14]([S:5][CH2:2][CH:3]=[CH2:4])=[CH:15][CH:16]=1)([CH3:9])([CH3:8])[CH3:7]

Participants

5

Reactant 3

HCID 13367Allyl MercaptanHCID 27639573-(Tert-Butoxy)-6-ChloropyridazineHCID 5360545Sodium

Product 1

HCID 21217662HCID 21217662, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

0.46 g(0.02 mol) of metallic sodium was dissolved in 30 ml of absolute methanol and then mixed with 1.99 ml(0.02 mol) of allylmercaptan. To this mixture was added 3.75 g(0.02 mol) of 3-(t-butoxy)-6-chloropyridazine. The reaction solution was refluxed for 24 hours and then treated according to the same manner as Example 1 to obtain the title compound as a pale yellow oil.

Workup

  1. temperatureThe reaction solution was refluxed for 24 hours
  2. additiontreated

Sources & evidence

ORD record
ord-9c6696d76fa54e988979e37f461f3190
Source dataset
uspto-grants-1999_08
Patent number
US05942511

Reaction notes

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