Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | O-Cresol | HCID 335 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 3-Chloro-6-[(prop-2-en-1-yl)sulfanyl]pyridazine | HCID 21217667 | — |
| Product | HCID 21217658 | HCID 21217658 | — |
Reaction Steps
0.23 g(0.01 mol) of metallic sodium was dissolved in 30 ml of dry o-cresol. To the resulting solution was added 1.87 g(0.01 mol) of 3-chloro-6-allylthiopyridazine. The reaction solution was stirred for 5 hours at 100±5° C. and then treated according to the same manner as Example 23 to obtain the title compound as a pale white needle crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05942511 |
|---|
| Source dataset | uspto-grants-1999_08 |
|---|
| ORD ID | ord-1722e8d2ed124226b4f09c7736fdd749 |
|---|
| Source note | uspto-grants-1999_08 |
|---|
