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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1586210Generated: November 4, 2026

Sodium Carbonate → HCID 135532380, compound

https://huagongshe.com/reaction/1586210

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium CarbonateHCID 10340—
ReactantHCID 135810727HCID 135810727—
ReactantHCID 178460562HCID 178460562—
SolventEthanolHCID 702—
ProductHCID 135532380HCID 13553238094.5%

Reaction Conditions

Temperature150 °C

Reaction Steps

9.6 g (0.028 mol) of 2,4-bis(2'-hydroxyphenyl)-6-phenyl-s-triazine, 25 ml (0.234 mol) of dimethylmethane phosphonate and 4.0 g (0.028 mol) of sodium carbonate are mixed and the mixture is heated to 150° C. After 2 hours the clear, pale red reaction solution is stirred into 150 ml of ethanol. The precipitate is filtered with suction, rinsed with 20 ml of ethanol and water and dried in an exsiccator, giving 9.4 g (94.1%) of the compound of formula ##STR7##

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05942564
Source datasetuspto-grants-1999_08
ORD IDord-67736a1518d24656bfd4276a1adab918
Source noteuspto-grants-1999_08