HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium methanethiolate → 1-(3,5-Dichlorophenyl)-2-(methylthio)ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium methanethiolate | HCID 4378561 | — |
| Reactant | 2-Bromo-1-(3,5-dichlorophenyl)ethan-1-one | HCID 12622490 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-(3,5-Dichlorophenyl)-2-(methylthio)ethanone | HCID 21852643 | 93.8% |
Reaction Steps
3.7 g (0.015 mol) of 1-(3,5-dichlorophenyl)-2-methylthio-1-ethanone are prepared by addition at 0° C. of 1.23 g (0.017 mol) of sodium methanethiolate in solution in 10 ml of methanol to 4.28 g (0.016 mol) of 2-bromo-1-(3,5-dichlorophenyl)-1-ethanone obtained above.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05945382 |
| Source dataset | uspto-grants-1999_08 |
| ORD ID | ord-267e4d7bd80c452e90d052f749abe405 |
| Source note | uspto-grants-1999_08 |