Diethyl Ether → HCID 14064683, compound

HRID 1586467Notes

Reaction equation

HRID 1586467 reaction equation
[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10][CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[NH:18][C:19](=[O:21])[CH3:20].C([O:24]CC)C>>[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10]([CH2:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[NH:18][C:19](=[O:21])[CH3:20])=[O:24]

Participants

3

Reactant 2

HCID 3283Diethyl EtherHCID 14064652HCID 14064652, compound

Product 1

HCID 14064683HCID 14064683, compound

Procedure

The title compound was prepared by the method of Example 3 using 1.80 g of the title product of Example 5 instead of the title product of Example 2. Trituration with diethylether gave 1.52 g of the title compound: m.p. 201-202.5° C. Anal. Calc'd. for C16H15N3O2S: C, 61.32; H, 4.82; N,13.41; S, 10.23. Found: C, 61.00; H, 4.90; N, 13.28; S, 10.50.

Sources & evidence

ORD record
ord-956b687a8b414bad89b5a21f73f0e0e7
Source dataset
uspto-grants-1999_08
Patent number
US05945425

Reaction notes

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