Diethyl Ether → HCID 14064683, compound

Participants

Reaction Steps

The title compound was prepared by the method of Example 3 using 1.80 g of the title product of Example 5 instead of the title product of Example 2. Trituration with diethylether gave 1.52 g of the title compound: m.p. 201-202.5° C. Anal. Calc'd. for C16H15N3O2S: C, 61.32; H, 4.82; N,13.41; S, 10.23. Found: C, 61.00; H, 4.90; N, 13.28; S, 10.50.

Provenance & Evidence