Diethyl Ether → HCID 13754162, compound

HRID 1586477Notes

Reaction equation

HRID 1586477 reaction equation
[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10][CH2:11][C:12]1[CH:17]=[C:16]([CH3:18])[CH:15]=[CH:14][C:13]=1[NH2:19].C(Cl)(Cl)Cl.C([O:26]CC)C>ClCCCl>[NH:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[S:10]([CH2:11][C:12]1[CH:17]=[C:16]([CH3:18])[CH:15]=[CH:14][C:13]=1[NH2:19])=[O:26]

Participants

5

Reactant 3

HCID 3283Diethyl EtherHCID 6212ChloroformHCID 13754141HCID 13754141, compound

Product 1

HCID 13754162HCID 13754162, compound

Reagents, catalysts & solvents 1

HCID 111,2-DichloroethaneSolvent

Procedure

The title compound was prepared by the method of Example 3 using 2.68 g of the title product of Example 25 instead of the title product of Example 2 and using 1,2-dichloroethane as solvent instead of chloroform. Trituration with diethyl ether gave 3.0 g of the title compound. Anal. Calc'd. for C15H15N3OS: C, 63.14; H, 5.30; N, 14.73; S, 11.23. Found: C, 61.44; H, 4.98; N, 14.35; S, 11.10.

Sources & evidence

ORD record
ord-8c65e92580684c4298f5a532856e6093
Source dataset
uspto-grants-1999_08
Patent number
US05945425

Reaction notes

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