Methacryloyl chloride → HCID 21216971, compound

HRID 1586522Notes

Reaction equation

HRID 1586522 reaction equation
[C:1]([C:5]1[N:13]=[C:12]2[C:8]([NH:9][CH:10]=[N:11]2)=[C:7]([NH2:14])[N:6]=1)(=[O:4])[CH:2]=[CH2:3].[C:15](Cl)(=O)C(C)=C>>[C:1]([C:5]1[N:13]=[C:12]2[C:8]([NH:9][CH:10]=[N:11]2)=[C:7]([NH2:14])[N:6]=1)(=[O:4])[C:2]([CH3:15])=[CH2:3]

Participants

3

Reactant 2

HCID 13528Methacryloyl chlorideHCID 21216970HCID 21216970, compound

Product 1

HCID 21216971HCID 21216971, compound

Procedure

All procedural steps and molar ratios were the same as those for the preparation of acryloyladenine, except that methacryloyl chloride was used instead of acryloyl chloride. The yield of MAD was 85%. The IR spectra showed the same bands as the IR spectra of AAD.

Sources & evidence

ORD record
ord-ca02235b9a554766925fdd4a6280bcc3
Source dataset
uspto-grants-1999_08
Patent number
US05945457

Reaction notes

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