HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloro-6-nitrophenol → 2-Amino-4,6-dichlorophenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloro-6-nitrophenol | HCID 11871 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-Amino-4,6-dichlorophenol | HCID 10699 | — |
Reaction Steps
The starting material, 2,4-dichloro-6-nitrophenol (260 g, 1 mole, 20% in water), was mixed with methanol (2 liters) and platinum oxide catalyst, and the resulting slurry was reacted with hydrogen at 4.2 kg/cm2 (60 psi) and room temperature.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05215925 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-dab98924dbbd47708dbb35d7c7b24aa1 |
| Source note | uspto-grants-1993_06 |