HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 15484978, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3,4-Dichlorophenyl isocyanate | HCID 7607 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Cyclopentanesulfonamide | HCID 4645983 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 15484978 | HCID 15484978 | 85.2% |
Reaction Steps
The general method of procedure A was followed with cyclopentanesulfonamide (3 g), acetone (200 ml), 1N sodium hydroxide (20 ml), and 3,4-dichlorophenyl isocyanate (3.6 g) dissolved in acetone (50 ml). After two hours, 1N HCl (20 ml) was added and the resulting solid diluted with water and collected. After drying at 5° C., 5.5 g of solid product were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05216026 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-f99622174c57423e97f5616f7ae57be9 |
| Source note | uspto-grants-1993_06 |