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HRID1586889

反应详情

EQUATION

反应方程式

HRID 1586889 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)N[C@@H](Cc1ccc(Cl)cc1)C(=O)O
HCID2734499

N-(tert-Butoxycarbonyl)-4-chloro-L-phenylalanine

C14H18ClNO4

结构：COC(=O)[C@H](N)C(C)(C)S.Cl
HCID12278508

Methyl 3-mercapto-D-valinate hydrochloride

C6H14ClNO2S

PRODUCTS

生成物

1
结构：COC(=O)[C@H](NC(=O)[C@H](Cc1ccc(Cl)cc1)NC(=O)OC(C)(C)C)C(C)(C)S
HCID131717962

未命名化合物

PROCEDURE

实验过程

The title compound was synthesized by coupling Nα -Boc-(p-chloro) phenylalanine (4.96 g, 16.5 mmol) to 3.6 g (18.2 mmol) of D-penicillamine methylester hydrochloride using the procedure described above in Example 19. The title compound was obtained as a white solid (6.2 g, 84.5%).

WORKUP

后处理

  1. customThe title compound was synthesized