HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Ethoxycarbonylbenzoyl chloride → HCID 19760190, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Ethoxycarbonylbenzoyl chloride | HCID 12276626 | — |
| Reactant | 7-Amino-1-methyl-1,3,4,5-tetrahydro-benzo[B]azepin-2-one | HCID 19760258 | — |
| Product | HCID 19760190 | HCID 19760190 | — |
Reaction Steps
Analogous to Example 1, from 7-amino-2,3,4,5-tetrahydro-1-methyl-2-oxo-1H-1-benzazepine was reacted with p-ethoxycarbonylbenzoyl chloride to yield ethyl p-[(2,3,4,5-tetrahydro-1-methyl-2-oxo-1H-1-benzazepin-7-yl)carbamoyl]benzoate, m.p. 184°-185° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05216148 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-e4fbc81f2b694f19854e569f77b7d61f |
| Source note | uspto-grants-1993_06 |