HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-5-hydroxypyridine → HCID 135492986, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-5-hydroxypyridine | HCID 14275 | — |
| Reactant | Lead dioxide | HCID 14793 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 135492986 | HCID 135492986 | 9.3% |
Reaction Steps
6-Methyl-3-hydroxypyridine (23.9 g, 0.219 moles), lead dioxide (98.3 g, 0.411 moles) and toluene (1 liter) were combined and refluxed for five hours. The hot solution was filtered and evaporated to dryness. The residue was refluxed with hexane and filtered while hot. The solution was evaporated to dryness giving the product as a yellow powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05216134 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-3279eea3e567486b942b6f8529b4ce90 |
| Source note | uspto-grants-1993_06 |