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HRID1586939

反应详情

EQUATION

反应方程式

HRID 1586939 的结构方程式

REACTANTS

反应物

2
结构：Nc1ccc(F)cc1
HCID9731

4-Fluoroaniline

C6H6FN

结构：CC1(C)CCC(C)(C)c2cc(C(=O)O)ccc21
HCID227638

5,5,8,8-Tetramethyl-5,6,7,8-tetrahydronaphthalene-2-carboxylic acid

C15H20O2

PRODUCTS

生成物

1
结构：CC1(C)CCC(C)(C)c2cc(C(=O)Nc3ccc(F)cc3)ccc21
HCID19760311

未命名化合物

收率 60.7%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCC.CCOC(C)=O
溶剂HCID21226206

未命名化合物

PROCEDURE

实验过程

In a manner analogous to Example 1, 2 g of 5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenecarboxylic acid and 1 g of 4-fluoroaniline were used to obtain 1.7 g of 4'-fluoro-5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthalenecarboxanilide in colorless crystals, m.p. 163°-165° C. (from ethyl acetate/hexane).