3-(4,6-Bis-trichloromethyl-s-triazin-2-yl) benzoylchloride → 2-[3-(4,6-Bis-trichloromethyl-s-triazin-2-yl)phenyl]-5-(3,4-dimethoxyphenyl)-1,3,4-oxadiazole

HRID 1586967Notes

Reaction equation

HRID 1586967 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([C:11]2[NH:15][N:14]=NN=2)[CH:6]=[CH:7][C:8]=1[O:9][CH3:10].[Cl:16][C:17]([Cl:38])([Cl:37])[C:18]1[N:23]=[C:22]([C:24]([Cl:27])([Cl:26])[Cl:25])[N:21]=[C:20]([C:28]2[CH:29]=[C:30]([CH:34]=[CH:35][CH:36]=2)[C:31](Cl)=[O:32])[N:19]=1>N1C=CC=CC=1>[Cl:27][C:24]([Cl:25])([Cl:26])[C:22]1[N:23]=[C:18]([C:17]([Cl:38])([Cl:16])[Cl:37])[N:19]=[C:20]([C:28]2[CH:29]=[C:30]([C:31]3[O:32][C:11]([C:5]4[CH:6]=[CH:7][C:8]([O:9][CH3:10])=[C:3]([O:2][CH3:1])[CH:4]=4)=[N:15][N:14]=3)[CH:34]=[CH:35][CH:36]=2)[N:21]=1

Participants

4

Reactant 2

HCID 145729223-(4,6-Bis-trichloromethyl-s-triazin-2-yl) benzoylchlorideHCID 178489170HCID 178489170, compound

Product 1

HCID 144732612-[3-(4,6-Bis-trichloromethyl-s-triazin-2-yl)phenyl]-5-(3,4-dimethoxyphenyl)-1,3,4-oxadiazole

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

5-(3,4-Dimethoxyphenyl)-tetrazole (20 pbw) and 3-(4,6-bis-trichloromethyl-s-triazin-2-yl)benzoyl chloride (44 pbw) are heated in 400 pbv of pyridine. The mixture is further processed as indicated above.

Sources & evidence

ORD record
ord-39a71f958c8945dfb8fb9737f851d678
Source dataset
uspto-grants-1993_06
Patent number
US05216158

Reaction notes

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