HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(4,6-Bis-trichloromethyl-s-triazin-2-yl) benzoylchloride → 2-[3-(4,6-Bis-trichloromethyl-s-triazin-2-yl)phenyl]-5-(3,4-dimethoxyphenyl)-1,3,4-oxadiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(4,6-Bis-trichloromethyl-s-triazin-2-yl) benzoylchloride | HCID 14572922 | — |
| Reactant | HCID 178489170 | HCID 178489170 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 2-[3-(4,6-Bis-trichloromethyl-s-triazin-2-yl)phenyl]-5-(3,4-dimethoxyphenyl)-1,3,4-oxadiazole | HCID 14473261 | — |
Reaction Steps
5-(3,4-Dimethoxyphenyl)-tetrazole (20 pbw) and 3-(4,6-bis-trichloromethyl-s-triazin-2-yl)benzoyl chloride (44 pbw) are heated in 400 pbv of pyridine. The mixture is further processed as indicated above.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05216158 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-39a71f958c8945dfb8fb9737f851d678 |
| Source note | uspto-grants-1993_06 |