HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trityl chloride → HCID 88465997, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trityl chloride | HCID 6456 | — |
| Reactant | Glycidol | HCID 11164 | — |
| Reactant | Potassium Bicarbonate | HCID 516893 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 88465997 | HCID 88465997 | 64.7% |
Reaction Steps
0.74 g of (RS)-glycidol and 2.8 g of trityl chloride in 5 ml of pyridine are reacted overnight. A solution of 2 g of potassium bicarbonate is then added while stirring. After evaporation, partition of the residue between water and methylene chloride and chromatography on silica gel with toluene there are obtained 2.25 g of (RS)-epoxy-1-O-tritylglycerol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05215972 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-576ed68887604420b8727e56cd3fce89 |
| Source note | uspto-grants-1993_06 |