Acrylonitrile → HCID 54184386, compound

HRID 1587542Notes

Reaction equation

HRID 1587542 reaction equation
[CH3:1][S:2][C:3]1[CH:9]=[CH:8][C:6](N)=[CH:5][CH:4]=1.[C:10](#[N:13])C=C>C(O)C>[CH3:6][C:8]1[CH:9]=[C:3]([CH:4]([CH3:5])[C:10]#[N:13])[S:2][CH:1]=1

Participants

4

Reactant 2

HCID 7855AcrylonitrileHCID 660384-(Methylthio)aniline

Product 1

HCID 54184386HCID 54184386, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Dissolve 4-(methylmercapto)aniline (25.7 g, 0.185 mol) and acrylonitrile (11.7 g, 0.22 mol) in ethanol (700 mL) and heat at reflux for 18 hours. Evaporate the solvent in vacuo and purify by distillation to give the title compound.

Workup

  1. temperatureheat
  2. temperatureat reflux for 18 hours
  3. customEvaporate the solvent in vacuo
  4. distillationpurify by distillation

Sources & evidence

ORD record
ord-076e48ce5a12453cab9547ba4ea35db7
Source dataset
uspto-grants-1993_06
Patent number
US05217964

Reaction notes

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