HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylonitrile → HCID 54184386, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | 4-(Methylthio)aniline | HCID 66038 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54184386 | HCID 54184386 | — |
Reaction Steps
Dissolve 4-(methylmercapto)aniline (25.7 g, 0.185 mol) and acrylonitrile (11.7 g, 0.22 mol) in ethanol (700 mL) and heat at reflux for 18 hours. Evaporate the solvent in vacuo and purify by distillation to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05217964 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-076e48ce5a12453cab9547ba4ea35db7 |
| Source note | uspto-grants-1993_06 |