Hydrochloric Acid → HCID 131717971, compound

HRID 1587548Notes

Reaction equation

HRID 1587548 reaction equation
[SH:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][N:9](C(OC(C)(C)C)=O)[CH2:10][CH2:11][CH2:12][N:13](C(OC(C)(C)C)=O)[CH2:14][CH2:15][CH2:16][N:17]([CH2:25][C:26]2[CH:31]=[CH:30][C:29]([SH:32])=[CH:28][CH:27]=2)C(OC(C)(C)C)=O)=[CH:4][CH:3]=1.[ClH:47]>>[ClH:47].[ClH:47].[ClH:47].[SH:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:8][NH:9][CH2:10][CH2:11][CH2:12][NH:13][CH2:14][CH2:15][CH2:16][NH:17][CH2:25][C:26]2[CH:27]=[CH:28][C:29]([SH:32])=[CH:30][CH:31]=2)=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 19757900HCID 19757900, compound

Product 1

HCID 131717971HCID 131717971, compound

Procedure

Dissolve 1,9-bis[(4-mercaptophenyl)methyl]-1,5,9-tri(t-butyloxycarbonyl)-1,5,9-triazanonane (4.75 g, 10 mmol) in saturated methanolic hydrochloric acid (100 mL). Stir for several hours and evaporate the solvent in vacuo to give the title compound.

Workup

  1. customevaporate the solvent in vacuo

Sources & evidence

ORD record
ord-1581db6d370e4e56a3cd580dfe8623fa
Source dataset
uspto-grants-1993_06
Patent number
US05217964

Reaction notes

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