HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 86746953, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | 1-(3-Pyridinyl)ethanone oxime | HCID 22279 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86746953 | HCID 86746953 | — |
Reaction Steps
7.4 g of 3-acetylpyridine oxime is dissolved in 80 cm3 of ethanol, 8 cm3 of benzyl bromide is added to it, with heating at reflux for 6 hours. The solvent is eliminated followed by crystallization from an ether/methanol mixture. 14.21 g of the expected product is obtained. m.p.=200°-201° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05219873 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-29a5bf5551d24054bc0acb824680845c |
| Source note | uspto-grants-1993_06 |