HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → HCID 86746955, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | HCID 85840682 | HCID 85840682 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86746955 | HCID 86746955 | — |
Reaction Steps
A mixture of 17.8 g of 3-propionyl pyridine oxime [(U.S. Pat. No. 3,004,979 (1961)] and 18 cm3 of benzyl bromide is maintained at reflux for 7 hours 30 minutes in 250 cm3 of ethyl acetate. After cooling and separating, 36.5 g of the expected product is obtained. m.p. 178°-180° C., recrystallized from an ethanol-ether mixture.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05219873 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-cfcd2ef009f548608c7f8261b5b2a4df |
| Source note | uspto-grants-1993_06 |