HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azidotrimethylsilane → HCID 57066699, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azidotrimethylsilane | HCID 78378 | — |
| Reactant | 367-44-2 | HCID 16688914 | — |
| Reactant | HCID 86746974 | HCID 86746974 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57066699 | HCID 57066699 | — |
Reaction Steps
A mixture of the epoxy alcohol (2R,3R) 3-(2,2-dimethoxyethyl)oxirane-methanol and azidotrimethylsilane in dichloromethane is reacted with diethylaluminum fluoride to obtain (2S,3S) 3-azido-5,5-dimethoxypentane1,2-diol: ##STR6##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05220003 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-d0a882f871a74f7bb804219f6323d5aa |
| Source note | uspto-grants-1993_06 |