HRID1588026

反应详情

EQUATION

反应方程式

HRID 1588026 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

3-Nitro-(1H-tetrazol-5-yl)benzene was dissolved in 200 ml of ethanol, treated with 1.7 g of 10% palladium/carbon catalyst, and hydrogenated on a Parr apparatus at 30 psi for 2 hours. The reaction mixture was filtered through Celite and concentrated to give 4.7 g of the title compound.

WORKUP

后处理

  1. filtrationThe reaction mixture was filtered through Celite
  2. concentrationconcentrated