HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
5-(3-nitrophenyl)tetrazole → HCID 178507542, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 5-(3-nitrophenyl)tetrazole | HCID 285129 | — |
| Katalysator | Palladium | HCID 23938 | — |
| Lösungsmittel | Ethanol | HCID 702 | — |
| Produkt | HCID 178507542 | HCID 178507542 | — |
Reaktionsschritte
3-Nitro-(1H-tetrazol-5-yl)benzene was dissolved in 200 ml of ethanol, treated with 1.7 g of 10% palladium/carbon catalyst, and hydrogenated on a Parr apparatus at 30 psi for 2 hours. The reaction mixture was filtered through Celite and concentrated to give 4.7 g of the title compound.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US05220018 |
| Quelldatensatz | uspto-grants-1993_06 |
| ORD ID | ord-8011f81aac654496807dfbdc36505afe |
| Quellennotiz | uspto-grants-1993_06 |