HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67855032, compound → HCID 19756852, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67855032 | HCID 67855032 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19756852 | HCID 19756852 | 137.9% |
Reaction Steps
3-Amino-N-(2-propylaminocarbonyl)phenylcarboxamide 3-Nitro-N-(2-propylaminocarbonyl)phenylcarboxamide (1.5 g) was dissolved in 150 ml of ethanol, treated with 850 mg of 10% palladium/carbon catalyst, and hydrogenated on a Parr apparatus at 30 psi for 10 minutes. The reaction mixture was filtered through Celite and concentrated to give the title compound (1.1 g) as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05220018 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-76165d9f4c394bee987027deb27da369 |
| Source note | uspto-grants-1993_06 |