HRID1588041

反应详情

EQUATION

反应方程式

HRID 1588041 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

3-Nitro-(2-methyltetrazol-5-yl)benzene (648 mg) was dissolved in 100 ml of ethanol, treated with 0.283 g of 10% palladium/carbon catalyst, and hydrogenated on a Parr apparatus at 30 psi for 15 minutes. The reaction mixture was filtered through Celite and concentrated to give 0.469 g of the title compound.

WORKUP

后处理

  1. filtrationThe reaction mixture was filtered through Celite
  2. concentrationconcentrated