HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-5-(3-nitrophenyl)-2H-tetrazole → HCID 178507542, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-5-(3-nitrophenyl)-2H-tetrazole | HCID 14045086 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178507542 | HCID 178507542 | 92.1% |
Reaction Steps
3-Nitro-(2-methyltetrazol-5-yl)benzene (648 mg) was dissolved in 100 ml of ethanol, treated with 0.283 g of 10% palladium/carbon catalyst, and hydrogenated on a Parr apparatus at 30 psi for 15 minutes. The reaction mixture was filtered through Celite and concentrated to give 0.469 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05220018 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-ed347d81b1bc43448fd747b6b78be16f |
| Source note | uspto-grants-1993_06 |