HCID 19756857, compound → HCID 19756861, compound

HRID 1588043Notes

Reaction equation

HRID 1588043 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]([C:10]2[N:14]=[N:13][C:12](=[O:15])[N:11]=2)[CH:7]=[CH:8][CH:9]=1)([O-])=O>C(O)C.[Pd]>[NH2:1][C:4]1[CH:5]=[C:6]([C:10]2[N:14]=[N:13][C:12](=[O:15])[N:11]=2)[CH:7]=[CH:8][CH:9]=1

Participants

4

Reactant 1

HCID 19756857HCID 19756857, compound

Product 1

HCID 19756861HCID 19756861, compoundYield 75%

Reagents, catalysts & solvents 2

HCID 23938PalladiumCatalystHCID 702EthanolSolvent

Procedure

3-Nitrophenyl-1,3,4-triazole-5-one (250 mg) was dissolved in 10 ml of ethanol, treated with 0.100 g of 10% palladium/carbon catalyst, and hydrogenated on a Parr apparatus at 25 psi for 5 minutes. The reaction mixture was filtered through Celite and concentrated to give 0.160 g of the title compound.

Workup

  1. filtrationThe reaction mixture was filtered through Celite
  2. concentrationconcentrated

Sources & evidence

ORD record
ord-d534ac4b48a9443e87873450797392af
Source dataset
uspto-grants-1993_06
Patent number
US05220018

Reaction notes

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