HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19756857, compound → HCID 19756861, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19756857 | HCID 19756857 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19756861 | HCID 19756861 | 75% |
Reaction Steps
3-Nitrophenyl-1,3,4-triazole-5-one (250 mg) was dissolved in 10 ml of ethanol, treated with 0.100 g of 10% palladium/carbon catalyst, and hydrogenated on a Parr apparatus at 25 psi for 5 minutes. The reaction mixture was filtered through Celite and concentrated to give 0.160 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05220018 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-d534ac4b48a9443e87873450797392af |
| Source note | uspto-grants-1993_06 |