HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 12011111, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | 4-Methoxybenzaldehyde | HCID 31244 | — |
| Reactant | HCID 45595268 | HCID 45595268 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 12011111 | HCID 12011111 | 230.8% |
Reaction Steps
To a solution of the amine 2.1 (2.51 g, 12.5 mmol) in 10 mL methanol were added p-anisaldehyde (1.5 mL, 12.5 mmol) and anhydrous sodium carbonate (1.3 g, 12.5 mmol). The mixture was stirred for 15 hours and was filtered through celite and concentrated to give 3.9 g of the corresponding p-anisaldehyde imine 2.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05220059 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-88025c7df7d14a08b720692de16b69dc |
| Source note | uspto-grants-1993_06 |