Phenol → HCID 14006101, compound

HRID 1588101Notes

Reaction equation

HRID 1588101 reaction equation
[OH-].[CH3:2][N+:3]([CH3:6])([CH3:5])[CH3:4].[C:7]1([OH:13])[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1>C(O)(C)C>[C:7]1([O-:13])[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1.[CH3:2][N+:3]([CH3:6])([CH3:5])[CH3:4]

Participants

4

Reactant 2

HCID 996PhenolHCID 60966Tetramethylammonium hydroxide

Product 1

HCID 14006101HCID 14006101, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

A commercially available 10% solution of tetramethylammonium hydroxide in methanol (manufactured by TOKYO KASEI CO.) was subjected to solvent exchange with isopropanol to produce a solution of tetramethylammonium hydroxide in isopropanol. To a 3.83 ml portion of the solution (2.24 mmoles of tetramethylammonium hydroxide) was added 0.211 g of phenol (2.24 mmoles) to produce a solution of tetramethylammonium phenolate in isopropanol.

Sources & evidence

ORD record
ord-10f1a51f89654e7d90431a47f764befe
Source dataset
uspto-grants-1993_06
Patent number
US05220079

Reaction notes

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