HuagongsheHuagongshe Chemistry Print Report · For research reference only
Guaiacol → HCID 67791299, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Guaiacol | HCID 460 | — |
| Reactant | HCID 19757443 | HCID 19757443 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67791299 | HCID 67791299 | 200% |
Reaction Steps
To 5.20 ml of a commercially available 10% tetramethylammonium hydroxide-methanol solution (manufactured by TOKYO KASEI; 5.05 mmole equivalents) was added 0.6264 g of guaiacol (5.05 mmoles), and methanol was removed under reduced pressure. To the residue was added 10 ml of isopropanol, and the alcohol was removed under reduced pressure again. Finally 5 ml of isopropanol was added to obtain about 7 ml of a tetramethylammonium-2-methoxyphenolate-isopropanol solution (containing 5.05 mmoles of guaiacol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05220079 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-3b0a4ab50fd444f88ef94a30cc98b25c |
| Source note | uspto-grants-1993_06 |