O-Cresol → HCID 67791299, compound

HRID 1588103Notes

Reaction equation

HRID 1588103 reaction equation
[OH-:1].[CH3:2][N+:3]([CH3:6])([CH3:5])[CH3:4].[CH3:7]O.[C:9]1(C)[C:14]([OH:15])=[CH:13][CH:12]=[CH:11][CH:10]=1>>[CH3:2][N+:3]([CH3:6])([CH3:5])[CH3:4].[CH3:7][O:1][C:9]1[CH:10]=[CH:11][CH:12]=[CH:13][C:14]=1[O-:15].[CH:14]([OH:15])([CH3:9])[CH3:13]

Participants

3

Reactant 2

HCID 335O-CresolHCID 19757443HCID 19757443, compound

Product 1

HCID 67791299HCID 67791299, compoundYield 200%

Procedure

To 5.28 ml of a commercially available 10% tetramethylammonium hydroxide-methanol solution (manufactured by TOKYO KASEI; 5.13 mmole equivalents) was added 0.555 g of o-cresol (5.13 mmoles). About 7 ml of a tetramethylammonium-2-methoxyphenolate-isopropanol solution (containing 5.13 mmoles of o-cresol) was obtained in the same manner as in Operation 1 in Example 4.

Sources & evidence

ORD record
ord-ab2fa835f6fe49a5908771cb6f935866
Source dataset
uspto-grants-1993_06
Patent number
US05220079

Reaction notes

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