1-Butanol → HCID 21893982, compound

HRID 1588184Notes

Reaction equation

HRID 1588184 reaction equation
C([NH:3][C:4](=[O:7])[CH:5]=[CH2:6])O.[C:8]1(C)C=C[C:11](S(O)(=O)=O)=[CH:10][CH:9]=1.[CH2:19]([OH:23])CCC>>[CH2:8]([O:23][CH2:19][C:5](=[CH2:6])[C:4]([NH2:3])=[O:7])[CH2:9][CH2:10][CH3:11]

Participants

4

Reactant 3

HCID 2631-ButanolHCID 6101p-Toluenesulfonic acidHCID 13543N-Methylolacrylamide

Product 1

HCID 21893982HCID 21893982, compound

Procedure

A reaction vessel equipped with a condenser, a stirrer, a thermometer, a nitrogen gas introducing tube and a dropping funnel was charged with 50.6 parts of N-methylolacrylamide and 148 parts of butanol and adjusted to pH 3.0 by adding p-toluenesulfonic acid. The reaction was started with refluxing and terminated for about four hours. The reaction product was neutralized with dimethylaminopropylmethacrylamide and butanol was removed under a reduced pressure to obtain 75 parts of n-butoxymethylacrylamide.

Workup

  1. customA reaction vessel equipped with a condenser, a stirrer
  2. additiona thermometer, a nitrogen gas introducing tube and a dropping funnel
  3. temperaturewith refluxing
  4. customterminated for about four hours
  5. customwas removed under a reduced pressure

Sources & evidence

ORD record
ord-37f8a73800034d458c2ab5ff7afa9e5e
Source dataset
uspto-grants-1993_06
Patent number
US05221589

Reaction notes

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