Triethylamine → HCID 54526280, compound

HRID 1588283Notes

Reaction equation

HRID 1588283 reaction equation
[NH:1]=[C:2]1[NH:6][C:5]([C:11]([F:14])([F:13])[F:12])([C:7]([F:10])([F:9])[F:8])[C:4](=[C:15]([F:20])[C:16]([F:19])([F:18])[F:17])[S:3]1.C(N(CC)CC)C.[C:28]([C:32]1[CH:40]=[CH:39][C:35]([C:36](Cl)=[O:37])=[CH:34][CH:33]=1)([CH3:31])([CH3:30])[CH3:29]>C1(C)C=CC=CC=1>[C:28]([C:32]1[CH:33]=[CH:34][C:35]([C:36]([NH:1][C:2]2[S:3][C:4](=[C:15]([F:20])[C:16]([F:17])([F:18])[F:19])[C:5]([C:7]([F:10])([F:9])[F:8])([C:11]([F:12])([F:13])[F:14])[N:6]=2)=[O:37])=[CH:39][CH:40]=1)([CH3:31])([CH3:29])[CH3:30]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 743724-tert-Butylbenzoyl chlorideHCID 178508427HCID 178508427, compound

Product 1

HCID 54526280HCID 54526280, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

In toluene (10 ml) were dissolved 2-imino-4,4-bis(trifluoromethyl)-5-(tetrafluoroethylidene)-1,3-thiazolidine (1.0 g) and triethylamine (0 4 ml), and 4-t-butylbenzoyl chloride (0.9 g) was gradually added thereto and the mixture was stirred at room temperature for 3 hours.

Workup

  1. additionwas gradually added

Sources & evidence

ORD record
ord-2a297d8b415e4beab00abed0ac055a77
Source dataset
uspto-grants-1993_06
Patent number
US05221685

Reaction notes

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