HRID1588291
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
CONDITIONS
反应条件
- 温度
- 103 °C
PROCEDURE
实验过程
In toluene (80 ml) were dissolved 2-imino-4,4-bis(trifluoromethyl)-5-(tetrafluoroethylidene)-1,3-thiazolidine (5.0 g) and triethylamine (1.5 ml), and a solution of 3-bromobenzoyl chloride (2.9 g) dissolved in toluene (10 ml) was gradually added thereto under cooling and the mixture was stirred at 103° C. for 3 hours.
WORKUP
后处理
- additionwas gradually added
- temperatureunder cooling