HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dichlorobenzene → HCID 19755403, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dichlorobenzene | HCID 4685 | — |
| Reactant | HCID 19755390 | HCID 19755390 | — |
| Product | HCID 19755403 | HCID 19755403 | — |
Reaction Steps
The product of Step 3 (400 mg) is heated in dichlorobenzene at 210° C. for 10 hours. Evaporation of the solvent and chromatography of the residue over silica gel using EtOAc-hexane yields ethyl 5-allyl-6-hydroxy-1,2,3,4-tetrahydrocarbazol-1-ylacetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05221678 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-6c100568967c43d38087f80889db7dc7 |
| Source note | uspto-grants-1993_06 |