HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylamide → Isooctyl Acrylate Acrylamide Vinyl Acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylamide | HCID 6579 | — |
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | Vinyl Acetate | HCID 7904 | — |
| Reactant | Isooctyl acrylate | HCID 165746 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Solvent | Ethylacetate methanol | HCID 21584119 | — |
| Product | Isooctyl Acrylate Acrylamide Vinyl Acetate | HCID 86608178 | — |
Reaction Steps
The procedures above were repeated this time employing 120.0 g. isooctyl acrylate, 8.0 g. acrylamide, 32.0 g. vinyl acetate, 0.32 g. benzoyl peroxide, 216.0 g. ethyl acetate and 24.0 g. methyl alcohol. The resulting polymer was diluted with the ethyl acetate/methyl alcohol mixture to 21.52% solids. The adhesive polymer had a measured inherent viscosity of 1.40 dl/g in ethyl acetate at a concentration of 0.15 g/dl. Its Brookfield viscosity was 2,300 centipoise.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05223261 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-91961685648c4baf8470fe805f28f874 |
| Source note | uspto-grants-1993_06 |