HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylamine → HCID 8625259, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylamine | HCID 6341 | — |
| Reactant | Ethylamine hydrochloride | HCID 11198 | — |
| Reactant | 4-(2-isothiocyanatophenyl)morpholine | HCID 5085456 | — |
| Solvent | Sodium Methoxide | HCID 10942334 | — |
| Product | HCID 8625259 | HCID 8625259 | — |
Reaction Steps
Reaction of 2-morpholinophenyl isothiocyanate (3.3 g) with ethylamine generated from ethylamine hydrochloride (12.18 g) and sodium methoxide [generated from sodium (3.5 g) and methanol (100 ml)] gave 1-ethyl-3-(2-morpholinophenyl)thiourea (m.p. 118°-120° C.) which was recrystallised from a 1:1 mixture of ethylacetate and hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05223498 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-34a640c0a7534c07bd35173916a62bc6 |
| Source note | uspto-grants-1993_06 |