HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 178476378, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 178521200 | HCID 178521200 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 178476378 | HCID 178476378 | — |
Reaction Steps
Reaction of 4-(2-[1-(2-hydroxyethyl)-2-imidazolidinylideneamino]phenyl)morpholine (3 g prepared as described in Example 175) in dichloromethane (20 ml) with acetic anhydride (0.86 g) yielded 4-(2-[1-(2-acetyloxyethyl)-2-imidazolidinylideneamino]phenyl)morpholine (m.p. 89°-91° C.) which was recrystallised from hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05223498 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-65b83e9cc8624136a9f57ceb80690172 |
| Source note | uspto-grants-1993_06 |