HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 2-Methyl-1-(5-chloro-2-morpholinophenyl)-3-(n-butyl)-2-thiopseudourea hydroiodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 1-(n-Butyl)-3-(5-chloro-2-morpholinophenyl)thiourea | HCID 18952277 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 2-Methyl-1-(5-chloro-2-morpholinophenyl)-3-(n-butyl)-2-thiopseudourea hydroiodide | HCID 18952297 | — |
Reaction Steps
A mixture of 1-(n-butyl)-3-(5-chloro-2-morpholinophenyl)thiourea (2.6 g), methyl iodide (1.4 g) and acetone (20 ml) was heated under reflux for 3 hours to give 2-methyl-1-(5-chloro-2-morpholinophenyl)-3-(n-butyl)-2-thiopseudourea hydroiodide (m.p. 130°-132° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05223498 |
| Source dataset | uspto-grants-1993_06 |
| ORD ID | ord-94bf1645f4a1483889e491817ed7974e |
| Source note | uspto-grants-1993_06 |